GCMS analysis results for sample AE12674, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12674 conducted on June 6, 2002.

NYC-WTC_000015006–000015015

Folder label: “GCMS X 5/30/02 A 6/1/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY3102\12674.D Vial: 19 Acq On 1 Jun 2002 5:42 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 11:38 2002 Quant Results File:GCMS0531 .RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 492618 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 1963248 40.00 ug/1 -0.02 17) Acenaphthene-dl0 20.99 164 938017 40.00 ug/1 -0.01 3 0) Phenanthrene-dl0 25.42 188 1436634 40.00 ug/1 -0.01 38) Chrysene-dl2 33.47 240 827901 40.00 ug/1 -0.03 44) Perylene-dl2 37.65 264 535601 40.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 23.14 209 210473 32.43 ug/L -0.01 Spiked Amount 40.000 Recovery 81.08% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.07 146 396 N.D. 5) 1,4-Dichlorobenzene 12.07 146 396 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 13.93 82 198 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.76 128 320 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenylphenylether 23.14 204 1515 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.14 168 416 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.49 178 381 N.D. (#) = qualifier out of range (m) = manual integration 12674.D GCMS0531.M Mon Jun 03 11:38:30 2002 Page 1

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GCMS analysis results for sample AE12672, June 2002 · Box DEP Box 15

NYC-WTC_000014943

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12672 conducted on June 6, 2002.

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