GCMS analysis report sample AE12094, June 2002

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GCMS laboratory analysis report for sample AE12094 showing unknown compounds and surrogate recovery data from June 6, 2002.

NYC-WTC_000014976–000014986

Folder label: “GCMS X 5/30/02 A 6/1/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY3102\12 0 94.D Vial: 17 Acq On 1 Jun 2002 3:44 am Operator: Morgan Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 11:36 2002 Quant Results File:"GCMS0531 .RES **- Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4' 12.07 152 505829 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 2029619 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 966467 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.42 188 1515749 40.00 ug/1 -0.01 38) Chrysene-dl2 33.47 240 912731 40.00 ug/1 -0.03 44) Perylene-dl2 37.65 264 564905 40.00 ug/1 -0.03

System Monitoring Compounds 28) TCMX 23.14 209 230386 34.45 ug/L -0.01 Spiked Amount 40.000 Recovery 86.13% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.41 74 432 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.07 146 398 N.D. 5) 1,4-Dichlorobenzene 12.07 146 398 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 2175 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.31 165 171 N.D. 25) Diethylphthalate 22.49 149 647 N.D. 26) 4-Chlorophenylphenylether 23.14 204 1327 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.14 168 591 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.48 178 1775 N.D. (#) = qualifier out of range (m) = manual integration 12094.D GCMS0531.M Mon Jun 03 11:36:44 2002 Page 1

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GCMS calibration data AE11284, DEP Labs, May 2002 · Box DEP Box 15

NYC-WTC_000014807

Calibration data for sample AE11284 analyzed using Method 508 on May 17, 2002.

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