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GCMS analysis results for sample AE12675, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12675 conducted on June 6, 2002.

NYC-WTC_000015016–000015026

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY3102\12675.D Vial: 20 Acq On 1 Jun 2002 6:41 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 11:39 2002 Quant Results File: GCMS0531 .RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 497156 40.00 ug/1 0.00 10) Naphthalene-d8 15.70 136 1983712 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 953771 40.00 ug/1 0.00 3 0) Phenanthrene-dl0 25.43 188 1449002 40.00 ug/1 0.00 38) Chrysene-dl2 33.48 240 853336 40.00 ug/i -0.03 44) Perylene-dl2 37.66 264 551309 40.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 23.13 209 221908 33.63 ug/L -0.02 Spiked Amount 40.000 Recovery 84.08% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.41 74 417 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichiorobenzene 12.08 146 106 N.D. 5) 1,4-Dichlorobenzene 12.08 146 106 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 13.93 82 325 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 945 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.29 165 174 N.D. 25) Diethylphthalate 22.48 149 497 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1408 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.14 168 685 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.49 178 364 N.D. (#) = qualifier out of range (m) = manual integration 12675.D GCMS0531.M Mon Jun 03 11:39:23 2002 Page 1

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