GCMS analysis results for sample AE12673, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12673 conducted on June 6, 2002.

NYC-WTC_000014996–000015005

Folder label: “GCMS X 5/30/02 A 6/1/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY3102\12673.D Vial: 18 Acq On 1 Jun 2002 4:43 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 11:37 2002 Quant Results File: GCMS0531.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev (Min)

1) l,4-Dichlorobenzene-d4 12.06 152 519011 40.00 ug/1 -0.01 10) Naphthalene-d8 15.69 136 2092277 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 997327 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.43 188 1560273 40.00 ug/1 0.00 38) Chrysene-dl2 33.47 240 947036 40.00 ug/1 -0.03 44) Perylene-dl2 37.66 264 598951 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.14 209 236160 34.23 ug/L -0.01 Spiked Amount 40.000 Recovery 85.57% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.42 74 176 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.08 146 183 N.D. 5) 1,4-Dichiorobenzene 12.08 146 183 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8). N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 331 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.33 165 355 N.D. 25) Diethylphthalate 22.48 149 1277 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1678 N.D. 2 7) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. ' 31) N-Nitrosodiphenylamine 23.14 168 840 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.42 178 666 N.D. (#) = qualifier out of range (m) = manual integration 12673.D GCMS0531.M Mon Jun 03 11:37:37 2002 Page 1

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GCMS analysis results for sample AE12672, June 2002 · Box DEP Box 15

NYC-WTC_000014943

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12672 conducted on June 6, 2002.

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