NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\MAY2302\12095.D Vial: 10
Acq On : 23 May 2002 8:59 pm Operator: Morgan
Sample : 5/21 bn Inst : 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: May 31 15:48 2002 Quant Results File:,GCMS0520 .RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator
Title : 209 625/TCLP calibration table
Last Update : Fri May 31 15:47:14 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0520
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.15 152 459970 40.00 ug/1 0.00
10) Naphthalene-d8 15.78 136 1670229m 40.00 ug/1 -0.01
17) Acenaphthene-diO 21.08 164 901703 40.00 ug/1 -0.01
3 0) Phenanthrene-dl0 25.52 188 1164864 40.00 ug/1 -0.01
38) Chrysene-dl2 33.57 240 604514 40.00 ug/1 -0.03
44) Perylene-dl2 37.79 264 410365 40.00 ug/1 -0.02
System Monitoring Compounds
28) TCMX 23.23 209 125937 27.79//Ug/L 0/00
Spiked Amount 40.000 Recovery = 1 69.47%
Target Compounds lue
2) N-nitrosodimethylamine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 • 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.57 149 358 N.D.
26) 4--Chlorophenylphenylether 23.23 204 555 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzene 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 23.23 168 180 N.D.
32) 4-Bromophenylphenylether 0.00 248 0 N.D.
3 3) Hexachlorobenzene 0.00 284 0 N.D.
34) Phenanthrene 25.53 178 306 N.D.
(#) = qualifier out of range (m) = manual integration
12095.D GCMS0520.M Fri May 31 15:48:45 2002 Page 1
NYC-WTC_000014818
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