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GCMS calibration data, DEP Labs, May 2002

Machine-extracted title · confidence 100%

Calibration results for gas chromatography mass spectrometry analysis of volatile organic compounds from May 31, 2002.

NYC-WTC_000014746–000014753

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY3 002\REF2.D Vial: 10 Acq On : 30 May 2002 10:56 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 11:21 2002 Quant Results File:GCMS0520 .RES *e- Quant Method : C:\PCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.63 178 652937 15.30 ug/1 99 36) Di-n-butylphthalate 27.41 149 900106 15.94 ug/1 100 37) Fluoranthene 29.12 202 716089 17.06 ug/1 95 39) Pyrene 29.79 202 746614 19.12 ug/1 92 40) Butylbenzylphthalate 31.92 149 343553 17.22 ug/1 94 41) Benzo(a)anthracene 33.42 228 489998 16.81 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.71 149 455107 17.35 ug/1 # 98 43) Chrysene 33.55 228 509648 17.70 ug/1 99 45) Di-n-Octylphthalate 35.45 149 613679 15.77 ug/1 # 91 46) Benzo(b)fluoranthene 36.51 252 378906 15.12 ug/1 97 47) Benzo(k)fluoranthene 36.57 252 417875 16.12 ug/1 97 48) Benzo(a)pyrene 37.46 252 278973 11.99 ug/1 # 95 49) Indeno(1,2,3-cd) pyrene 41.62 276 291617 13.04 ug/1 97 50) Dibenz(a,h)anthracene 41.68 278 250892 14.04 ug/1 95 51) Benzo (g,h,i)perylene 42.80 276 258841 14.48 ug/1 97

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0520.M Fri May 31 11:22:35 2002 Page 2

NYC-WTC_0000 14752

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NYC-WTC_000014752Source: NYC Law Department, mirrored locally

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