GCMS blank analysis results, sample AE12093, May 2002

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GCMS blank analysis report for sample AE12093 dated 05/31/2002 showing all measured organic compounds below minimum reporting limits (MRL) of 2.0 micrograms.

NYC-WTC_000014733–000014741

Folder label: “GCMS X 5/29/02 A 5/30/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY3002\LB.D Vial: 8 Acq On : 30 May 2002 8:57 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 11:07 2002 Quant Results File :„GCMS0520. RES —er Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 12.07 152 549722 40.00 ug/1 -0.07 10) Naphthalene-d8 15.70 136 2200939 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1044424 40.00 ug/1 -0.09 30) Phenanthrene-dlO 25.43 188 1628060 40.00 ug/1 -0.10 38) Chrysene-dl2 33.48 240 989269 40.00 ug/1 -0.13 44) Perylene-dl2 37.66 264 616763 40.00 ug/1 -0.15

System Monitoring Compounds 28) TCMX 23.13 209 181040 34.49 ug/L -0.10 Spiked Amount 40.000 Recovery 86.23% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.42 74 228 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2*-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 361 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.49 149 601 N.D. 26) 4-Chlorophenylphenylether 23.12 204 1242 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.14 168 167 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.42 178 941 N.D. (#) = qualifier out of range (m) = manual integration LB.D GCMS0520.M Fri May 31 11:08:10 2002 Page 1

NYC-WTC_000014734

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GCMS blank analysis for sample AE12163, May 2002 · Box DEP Box 15

NYC-WTC_000013775

Laboratory report documenting GCMS analysis of sample AE12163 conducted on May 29, 2002.

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