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GCMS analysis results, sample AE12636, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12636 including surrogate recovery data on June 7, 2002.

NYC-WTC_000014641–000014650

Folder label: “GCMS X 5/28/02 A 6/4/02

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Scanned page image, NYC-WTC_000014646
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NYC 9/11 Public Portal Document LSC Area Percent Report

• ‘Data File C:\HPCHEM\l\DATA\JUN0302\12536 .D Vial: 17 Acq On 4 Jun 2002 12:59 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.072 326 .330 343 rBV 24606 68510 1.97% 0.366% 2 12.066 760 765 783 rBV 1028029 2507362 71.98% 13.394% 3 15.692 1154 1160 1176 rBV 1609531 3408562 97.86% 18.208% 4 20.989 1731 1737 1752 rBV 1694278 3483237 100.00% 18.607% 5 23.128 1960 1970 1983 rBV 827850 1740478 49.97% 9.297% 6 25.423 2214 2220 2232 rBV2 1583340 3460229 99.34% 18.484% 7 25.561 2232 2235 2248 rVB2 11459 37453 1.08% 0.200% 8 33.474 3090 3097 3112 rBV2 1030556 2361356 67.79% 12.614% 9 37.651 3544 3552 3565 rBV2 580101 1653061 47.46% 8.830%

Sum of corrected areas: 18720248 12536.D GCMS0531.M Tue Jun 04 11:51:41 2002

NYC-WTC_000014646

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NYC-WTC_000014646Source: NYC Law Department, mirrored locally

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