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GCMS analysis results for sample AE12570, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12570 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014680–000014689

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\JUN0302\12570.D Vial: 21 Acq On 4 Jun 2002 4:56 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.068 325 329 331 rBV 26059 48116 1.34% 0.250% 2 8.114 331 334 343 rVB 22354 55130 1.54% 0.286% 3 12.061 759 764 786 rBV 999559 2556182 71.37% 13.263% 4 15.696 1153 1160 1176 rBV 1592878 3451686 96.37% 17.909% 5 20.994 1730 1737 1754 rBV 1660445 3554420 99.24% 18.442% 6 23.133 1958 1970 1982 rBV 824822 1720934 48.05% 8.929% 7 25.428 2213 2220 2231 rBV2 1639447 3581548 100.00% 18.583% 8 27.411 2430 2436 2442 rBV 21219 41120 1.15% 0.213% 9 33.470 3089 3096 3114 rBV2 1081772 2511448 70.12% 13.031% 10 37.656 3544 3552 3567 rBV2 604199 1752825 48.94% 9.095%

Sum of corrected areas: 19273409 12570.D GCMS0531.M Tue Jun 04 11:52:32 2002

NYC-WTC_000014685

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NYC-WTC_000014685Source: NYC Law Department, mirrored locally

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