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GCMS analysis results for sample AE12734, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12679 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015121–000015130

Folder label: “GCMS X 5/31/02 A 6/3/02

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Scanned page image, NYC-WTC_000015126
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\JUN0302\12734.D Vial: 12 Acq On 3 Jun 2002 8:02 pm Operator: Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.076 327 330 343 rBV2 15600 46862 1.36% 0.251% 2 12.069 759 765 782 rBV 998515 2486323 72.00% 13.316% 3 15.696 1154 1160 1176 rBV 1608475 3382892 97.96% 18.117% 4 20.993 1730 1737 1749 rBV 1693045 3451934 99.96% 18.487% 5 23.132 1962 1970 1984 rBV 834844 1718301 49.76% 9.203% 6 25.427 2213 2220 2231 rBV2 1638188 3453465 100.00% 18.495% 7 25.564 2231 2235 2249 rVB 11053 40220 1.16% 0.215% 8 33.478 3090 3097 3113 rBV2 1008137 2411665 69.83% 12.916% 9 37.655 3544 3552 3571 rBV2 573725 1680446 48.66% 9.000%

Sum of corrected areas: 18672108 12734.D GCMS0531.M Tue Jun 04 09:04:23 2002

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NYC-WTC_000015126Source: NYC Law Department, mirrored locally

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