GCMS analysis results, sample AE12476, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12476.D Vial: 18 Acq On : 29 May 2002 11:56 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemst at ion Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L Peak Number 13 Ethyl Chloride Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

5.01 0.50 ug/L 365974 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethyl Chloride 64 C2H5C1 000075-00-3 9 2 Flucytosine 129 C4H4FN30 002022-85-7/7 3 Flucytosine 129 C4H4FN30 002022-85-7 7 4 2-Chloro-4-aminopyrimidine 129 C4H4C1N3 007461-50-9 5 Abundance Scan 329 (5.012 min): 12476.D (-325) (-) m/z 128.90 00.00% 12.9

mfe-> 5000

0+ — 33 48

10 20 30 40 50 60 70 80 90 79

............. 1 111'1111 11'' 11' 88

100 110 120 130 4.60 4.80 m/z 126.90 A 5.00 5.20 5.40 79.69% Abundance #107943: Ethyl Chloride 23

64 5000 4.60 4.80 5.00 5.20 5.40 | 49 m/z 130.90 32.90% 35

n/z-> 01 - 10 20 30 15 1 Ht 40 50 60 70 80 90 100 'll6 120 130 T

Abundance #121819: Flucytosine 129

4.60 4.80 5.00 5.20 5.40 5000 m/z 78.90 30.76%

86 43 53 58 67 74 1931 113 0* 1 । | । ri i । i i i i । i i i i I‘l l'l prillj mpt43l i i [ rtti | ■ ■ ■ i |‘l . . rt । ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #58311: Flucytosine 12.9 4.60 4.80 5.00 5.20 5.40 m/z 48.10 24.82? 5000 86 59 31 43 , 101 0 ‘r11 16' 1111251 h ।1674. 1 93 1.113.... I „ 53 ■ I’l'l'ift ।—tr /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 4.60 4.80 5.00 5.20 5.40

12476.D 052202.M Mon Jun 03 11:34:13 2002 Page 16

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