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GCMS reference results for VOCs, sample AE12326, June 2002

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Laboratory report showing GCMS reference analysis data for volatile organic compounds in sample AE12326 on June 4, 2002.

NYC-WTC_000014379–000014383

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\052902\REFA1.D Vial: 15 Acq On : 29 May 2002 9:30 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 03 11:28:31 2002 Quant Results File: 052202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 29 08:47:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.49 202 7302631 14.34 ug/L 98 3 8) Pyrene 27.13 202 7560557 17.76 ug/L 99 39) Butylbenzylphthalate 29.48 149 2030965 11.15 ug/L 99 4 0) Benzo(a)anthracene 30.74 228 4821027 15.00 ug/L 100 41) Bis(2-ethylhexyl)phthalate 31.34 149 2089961 8.82 ug/L 98 42) Chrysene 30.83 228 5619268m 15.22 ug/L 44) Di-n-octylphthalate 33.19 149 1699392 6.10 ug/L 97 4 5) Benzo(b)fluoranthene 33.70 252 3406859 13.29 ug/L 99 46) Benzo(k)fluoranthene 33.77 252 4798311 16.71 ug/L 98 47) Benzo(a)pyrene 34.50 252 2323023 10.13 ug/L 98 48) Indeno(l,2,3-cd)pyrene 37.32 276' 1375893 9.00 ug/L 95 4 9) Dibenz(a,h)anthracene 37.44 278 2175466 12.94 ug/L 99 50) Benzo (g,h, Dperylene 38.06 276 2552534 14.30 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed REFAI.D 052202.M Mon Jun 03 11:29:04 2002 Page 2

NYC-WTC_000014382

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NYC-WTC_000014382Source: NYC Law Department, mirrored locally

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