GCMS analysis results, sample AE12325, June 2002

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C: \MSDCHEM\1\DATA\ 052902\12325.D Vial: 13 Acq On : 29 May 2002 7:51 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Methane, chlorodifluoro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.79 2.49 ug/L 1784620 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methane, chlorodifluoro- 86 CHC1F2 000075-45-6 B 2 Propiolonitrile 51 C3HN 001070-71-93 3 2-p-Nitrobenzoyl-1,3,5-tribenzyl... 569 C33H31NO8 1000129-85-6 2 4 2-Butyne-1,4-diol, diformate 142 C6H604 036677 -73-3 1 Abundance Scan 120 (3.784 min): 12325.D (-117) (-) m/z 51.05 100.00% 51 37 5000 47 83

42 86 ■ i ' ■ ■ ■ i 1 1 1 1 I 1 1 1 1 i ' 1 58 3.40 3.60 3.80 4.00 4.20 0+ qp "T THIIPmgT JI...... [ m/z 37.10 55.22% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12363: Methane, chlorodifluoro- 51

5000 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i • ■ ■ • i ■ 1 3.40 3.60 3.80 4.00 4.20 31 35 67 m/ z 82.95 44.23% | 70 8588 54 niz-> 0! 131619 24 TTTgT 111..,28,,11187. 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 t n-[TrT 111 i 11 | 11111 I 111 | 11 | 11 i 11 1111 111 | 11 | | 11

Abundance #12371: Propiolonitrile 51 3.40 3.60 3.80 4.00 4.20 5000 m/z 47.10 39.56%

miz-> 01 5+12.+18,.428,32.3,+,47, 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 S"r Abundance #12372:2-p-Nitrobenzoyl-1,3,5-tribenzyl-.alpha.-d-ribose 51 3.40 3.60 3.80 4.00 4.20 m/z 84,00 30.77% 5000

41 45 0: “ |1 “ ' I " irpir 111 n ■ | ■ 11111 ■ 111111 ■ । [ I II 48 15558 6265 69 -Hhmmmmmmmp ' i ‘ • i • ■ ■ ■ i ■ ■ ■ ■ i • ■ ' ■ i 1 ■ m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00 4.20

12325.D 052202.M Mon Jun 03 10:53:23 2002 Page 8

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