GCMS analysis results, sample AE12325, June 2002

NYC 9/11 Public Portal Document Library searcn Lompoura Keporu

Data File : C:\MSDCHEM\1\DATA\052902\12325.D Vial: 13 Acq On : 29 May 2002 7:51 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 Propanal, 2-methyl-2-(methy... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.87 3.23 ug/L 2314700 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Propanal, 2-methyl-2-(methylsulf... 149 C5H11NO2S 007635-32-7 10 2 2-Imidazolidinone 86 C3H6N20 000120-93-47 3 1-Propyne, 1-(methylthio)- 86 C4H6S 022174-51-2 7 4 2-Imidazolidinone 86. C3H6N20 000120-93-4 7 Abundance Scan 135 (3.872 min): 12325.D (-133) (-) m/z 86.00 7100.00% 85

5000 49

82 38 42 70 ***’I*’’*I’*’I*’**}’’ 3.60 3.80 4.00 4.20

m/z-> Ot - m ■■i■ “ 'i •" 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ i ‘• i “' m/z 49.10 48.05% Abundance #34648: Propanal, 2-methyl-2-(methylsulfinyl)-, oxime 41 86

5000 28 3.60 3.80 4.00 4.20 15 31 45 64 69 m/z 82.00 25.47% 01WTIUTIT 38 mM -H 34H , Tp76 189 Tmmmpnr niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108253: 2-Imidazolidinone 33 86 AAA 3.60 3.80 4.00 4.20 5000 m/z 42.10 20.69% 42 '_______________ 27 miz-> 0 ' I " " I “ ‘ ’I " • ‘ I " ' ‘ I 1 1 ‘ ■ ■ 39, 1545,... .71....a tH i n.. 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 TI00011137

Abundance #34894:1-Propyne, 1-(methylthio)- .... 1 .... 1 .... 1 .... J ... . 85 3.60 3.80 4.00 4.20 71 m/z 88.00 20.69% 45

5000

27 39 JLPPYahm 0 + 1.303336 1,42, 14851$15659 64 6 +1+ Hipinyer 111111» H ip 1att m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 420

12325.D 052202.M Mon Jun 03 10:53:23 2002 Page 9

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