GCMS sample AE12765 results, June 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\060402\12765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan *6 Library : C:\DATABASE\NIST98.L Peak Number 3 Methane, chlorodifluoro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 3.75 5.51 ug/L 3548110 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methane, chlorodifluoro- 86 CHC1F2 000075-45-6/4 2 Propiolonitrile 51 C3HN 001070-71-9 3 3 2-p-Nitrobenzoyl-1,3,5-tribenzyl... 569 C33H31NO8 1000129-85-6 2 4 1,1,2-Trifluoroethane 84 C2H3F3 000430-66-0 2 Abundance Scan 114 (3.749 min): 12765.D (-113) (-) m/z 51.10 00.00% 51 84 88 5000 48

3538 42 3.40 3.60 3.80 4.00 0! m odayalpalla/ mTTTTTTTTTTTT m/z 84.00 53.15% i ■ ■" i" " i" miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12363: Methane, chlorodifluoro- 51

5000 3.40 3.60 3.80 4.00 31 35 67 m/z 88.00 48.54%

niz-> Abundance Ot —138, 131619 24 —47+ 54 .i-r. Hi । ■. 111 ■.. 11. । 8588 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 l■■|

#12371: Propiolonitrile 51 | 70 | !l 11| ■ ■ । | ■.. ■ [ “ ouuWyep 3.40 3.60 3.80 4.00 5000 m/z 48.10 39.08%

n/z-> 01 5 +12.+18,4428,32..38,+447, 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 l>■ i>•>•। i ‘i*■i" *•i‘ i" " i ■' • • i • * PA— Abundance #12372:2-p-Nitrobenzoyl-1,3,5-tribenzyl-.alpha.-d-ribose 51 3.40 3.60 3.80 4.00 m/z 42.10 18.92% 5000

45 411

n/z—> 0 ----++44 5558 6265,69 I 1 | I I I I | I fl I | I I I ! | I 1 1 ■ | 11 I I | I 1 1 r| I i r< | 1 1 1 1 1 : I

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00

12765.D 060302.M Wed Jun 05 14:05:20 2002 Page 6

NYC-WTC_000015546