GCMS sample AE12765 results, June 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\060402\12765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Crotonic acid Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.87 2.20 ug/L 1413010 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua 1 Crotonic acid 86 C4H602 003724-65-0 3 2 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0/4 3 Borane, trifluoro- 68 BF3 007637-07-2 2 4 Krypton 84 Kr 007439-99-9 2 Abundance Scan 134 (3.867 min): 12765.D (-133) (-) m/z 86.00 100.00% 49 85

5000 38 35 42 3.60 3.80 4.00 4.20 ob■ “ ■ i “ ■ ■ i “■ i ■ ■ ■ ■ i •" ■ i ‘" i" ■ - -p m/z 84.00 97.37% n/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116766: Crotonic acid 41 83

5000 69 3.60 3.80 4.00 4.20 27 38 45 m/z 49. 10 84.21% 15 0bi "5" „1318,,241 13134 4+ 5053 5760 66 2mp —mp ■ I■'■ 'I'11 '11"11'' n/z-> 0 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34862: Imidazol, 4-fluoro- 83

3.60 3,80 4.00 4.20 5000 m/z 38.05 22.04%

59

0b »• 1''' u • ‘ “ I " ' ■ 11' ■ • I " " I • ‘ " I — Wr iz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12321: Borane, trifluoro- 49 3.60 3.80 4.00 4.20 m/z 48.10 20.72% 5000

11 19 TE—OTTTT TOPmPMP) 30 38 68 W 0b /z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

12765.D 060302.M Wed Jun 05 14:05:23 2002 Page 7

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