GCMS analysis results, sample AE12324, June 2002

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Gas chromatography mass spectrometry results for sample AE12324 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014303–000014329

Folder label: “GCMS X 5/24/02 A 5/29/02”

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NYC 9/11 Public Portal Document Library search compound Report Data File : C:\MSDCHEM\l\DATA\052902\12324.D Vial: 12 Acq On : 29 May 2002 7:03 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 1,2,3-Butatriene, 1-chloro- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 3.99 0.70 ug/L 472097 1,4 -Diehl orobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,2,3-Butatriene, 1-chloro- 86 C4H3C1 020658-21-3 9/ 2 l-Buten-3-yne, 1-chloro-, (Z)- 86 C4H3C1 020374-90-7 9 3 l-Buten-3-yne, 1-chloro-, (E)- 86 C4H3C1 020374-91-8/4 4 l-Buten-3-yne, 1-chloro-, (Z)- 86 C4H3C1 020374-90-7 4 Abundance Scan 154 (3.984 min): 12324.D (-153) (-) m/z 51.10 100.00% 47 51 43 86 5000

36 40 58 3.60 3.80 4.00 4.20 4.40 0- TTTTp-rrTTTTTTTrTTTT 11T HH 1 * i1 * ‘ I ' ' “ I “ “ I ' ' ‘ ' 1 1 “ 1 I “ Im m/z ... 47.00 85.88% m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12404:1,2,3-Butatriene, 1-chloro- 51 86

5000 3.60 3.80 4.00 4.20 4.40 m/z/ 86.00 59.70%

Of “ i “ “ p * * i j111 * i *11TTT1 “ 11 “1H +TTThmmt 189. -rp-r 60 miz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 v TM Abundance #12406: 1-Buten-3-yne, 1-chloro-, (Z)- 51 86 1 i ■ ‘ । i1 ■ ■ 1 । ■ r 1 ■ । 1 1 1 11 *1 3.60 3.80 4.00 4.20 4.40

k 5000 m/z 43.10 58.95%

26 30 37 43 48 60 63 71 74 83. 39 O-r i * | ><> i | H * I j i i 1 i | 1 1 I r riI I[i I I I —TTTT r| rl i l | ITTTf. . 1 . | I I > l'| > 1 > I | 4 r' p ■ ITITT W niz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12408:1-Buten-3-yne, 1-chloro-, (E)- ■ i ‘ ■ 1 ■ i • • ‘ ■ i ' 1 • ■ i ■ ' 51 86 3.60 3.80 4.00 4.20 4.40 m/z 84.00 32.39% 5000

TTummumummmmmomtf +89—7T-p-T 1 60

/z-> oR 15 i ■ •" i “ “ I' “11 “ “ f1 “ 111111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20 4.40

12324.D 052202.M Mon Jun 03 10:52:06 2002 Page 10

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