GCMS analysis results for sample AE12472, June 2002

NYC 9/11 Public Portal Document ulJLaly searci tompounu Kepor L

Data File : C:\MSDCHEM\1\DATA\052802\12472.D Vial: 10 Acq On : 28 May 2002 9:38 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan **** Library : C:\DATABASE\NIST98.L Peak Number 16 Phenanthrene-diO Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

23.07 0.27 ug/L 255590 Phenanthranene - dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 72* 2 Phosphonic acid, (3-methyl-3-pen... 188 C8H13O3P 022152-34-7 59 3 Anthracene-diO- 188 C14D10 001719-06-8 50 r 4 Pentacyclo[7.3,1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 45 Abundance Scan 3402 (23.068 min): 12472.D (-3395) (-) m/z 188.10 100.00%| 188

50001

80 94 22.80 23.00 23.20 23.40 niz-> 0 ------- 43 57 66 ITT 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 LH m/z 94.10 16.75 Abundance #79827: Phenanthrene-d10 108

5000 22.80 23.00 23.20 23.40 80 m/z 189.00 16.41 94 160 30 42 52 66 , 11 108118 132 146 h, 170179. ,I 0 | I . . . 1 . . . 1 | . . I 1 | I I ! I | H I ! | I 111 11 > H | I Tmmm n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79704: Phosphonic acid, (3-methyl-3-penten-1-ynyl)-, dime... 188 ........... 7 V .............. .......... .. 22.80 23.00 23.20 23.40 5000 77 m/z 80.00 14.61% 62 35 47 91 109 155

l aloksanoamapls. 18 141 . । 173 0- I ..... .,’1018237 11 T’TT miz-> 10 20 30 40 50 60 70 80 90-100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- JI 188 22.80 23.00 23.20 23.40 m/z 184.10 13.87%

5000

„ 80 — 94 2," O0 160 17 30 42 52 ° , , 108118 132 146 II 170179, 0J niz—> 10 2030405060 70 8090 100110120130140150160170 180 190 22.80 23.00 23.20 23.40

12472.D 052202.M Thu May 30 10:42:00 2002 Page 19

NYC-WTC_000014077