NYC 9/11 Public Portal Document
Llorary searen compound Keport
Data File : C:\MSDCHEM\1\DATA\052802\12287.D Vial: 6
Acq On : 28 May 2002 6:22 pm Operator: McLean
Sample : 5/24 ad Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 20 IH-Pyrrole, 1,1',1''-boryli... Concentration Rank 17
R.T. EstConc Area Relative to ISTD R.T.
34.90 0.27 ug/L 115124 Perylene-d12 34.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1H-Pyrrole, 1,1' , 1" -borylidynet. . . 209 C12H12BN3 018899-90-6 7
2 Quinoline, 2-(1-methyl-lH-imidaz... 209 C13H11N3 002552-97-8 7
3 4-Methylbenzylidene-4-methylaniline 209 C15H15N 016979-20-77
4 2-Propen-1-one, 1,3-diphenyl- 208 C15H120 000094-41-7 7
Abundance Scan 5416 (34.901 min): 12287.D (-5413) (-) m/z 2 0 7.00 100.00%
207
5000 116
260
uMrshawaluth
44 147 281
73 34.60 34.80 35.00 35.20
O-T 1 ■ i' ■ ■ ■ i' ■' • i ■ ■ i ■ ‘■ i ■ ' ■ ■ i ■ ■' ■ i ■ ■ ■ ■ i' ■ ■ i1 1 ■ ■ i11
I
m-r-p-r m/z 208.00 66.75%
l
nz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #85124: 1H-Pyrrole, 1,1’,1"-borylidynetris-
208
5000 “rnnt
34.60 34.80 35.00 35.20
143 m/z 209.00 51.54%
116
, 63 76 89
iz->
0
20
27,4,51,44.78.4,104 +,128.4.1551714...
40 60 80 100 120 140 160 180 200 220 240
1 ■ I ■ ■' ■ i •' ■ ■ i' ‘
260 280
■ i ■1
Abundance
5000
#85119: Quinoline, 2-(1 -methyl-1 H-imidazol-5-yi)-
208
LMahdasusn
34.60 34.80 35-00 35.20
m/z 260.10 48.93%
77 128I 155
102 140
OA [ 11111111 11 ■ । ,44%
1114
.. J I I, 168 181193
T * I' • ‘ ‘ I ‘ 1 • * 1 ‘ ‘ 1 ' I *1
miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #85332:4-Methylbenzylidene-4-methylaniline ----1
209 34.60 34.80 35.00 35.20
m/z 116.10 41.81%
50001 91
65
27 39 51 | 77 .
103 118,30 149 165178 194 , 14
0- Tm ■. . । , . . . ( i i-n -| i i ■ i । i i
n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20
12287.D 052202.M Thu May 30 10:40:38 2002 Page 23
NYC-WTC_000014031
OCR can misread numbers and units. Confirm readings against the page image before using them.