GCMS quantitative results for sample AE11602, May 2002

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Data File : C:\MSDCHEM\l\DATA\052802\524REFl.D Vial: 4 Acq On : 28 May 2002 4:45 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 30 10:35:49 2002 Quant Results File: 052202.RES g*.*

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integratbr) Title : 508 Modified GC/MS scan Last Update : Wed May 29 08:47:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.49 202 8044674 15.80 ug/L 98 3 8) Pyrene 27.13 202 8386919 19.14 ug/L 99 39) Butylbenzylphthalate 29.48 149 2258991 12.04 ug/L 98 4 0) Benzo(a)anthracene 30.74 228 5355919 16.19 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.34 149 2371028 9.72 ug/L 99 42) Chrysene 30.83 228 6335106m 16.67 ug/L 44) Di-n-octylphthalate 33.19 149 2050453 7.54 ug/L 99 45) Benzo(b)fluoranthene 33.70 252 4002348 15.98 ug/L 99 46) Benzo(k)fluoranthene 33.77 252 5120788 18.26 ug/L 99 47) Benzo(a)pyrene 34.50 252 2565189 11.45 ug/L 99 48) Indeno(l,2,3-cd)pyrene 37.32 276 1451075 9.72 ug/L 95 49) Dibenz(a,h)anthracene 37.44 278 2010235 12.24 ug/L 98 50) Benzo(g,h,i)perylene 38.06 276 2347034 13.46 ug/L 98

(#) = qualifier out of range (m) = manual integration {+) = signals summed 524REF1.D 052202.M Thu May 30 10:36:17 2002 Page 2 -a

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