Reference standard analysis data for gas chromatography-mass spectrometry testing of volatile organic compounds on May 22, 2002.
NYC-WTC_000013081–000013088Folder label: “GCMS X 5/21/02 A 5/21/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document quantitaton keport (1 Revlewed)
Data File C:\MSDCHEM\1\DATA\0 52102\REF1.D Vial: 11 Acq On 21 May 2002 9:29 pm Operator: Mclean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 22 12:03:35 2002 Quant Results File: 052202.RES
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last update : Wed May 22 12:00:55 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Compound R.T. Qlon Response Cone Unit Qvalue 3 6) Fluoroanthene 26.50 202 8579366 15.89 ug/L 98 38) Pyrene 27.13 202 8967781 16.83 ug/L 99 39) Butylbenzylphthalate 29.48 149 2749917 12.06 ug/L 97 4 0) Benzo(a)anthracene 30.74 228 6371299 15.84 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.35 149 3218988 10.85 ug/L 97 42) Chrysene 30.84 228 7354444m 15.91 ug/L 44) Di-n-octylphthalate 33.20 149 3456555 10.00 ug/L 100 45) Benzo(b)fluoranthene 33.70 252 5048985 15.87 ug/L 99 46) Benzo(k)fluoranthene 33.78 252 6140068 17.22 ug/L 100 4 7) Benzo(a)pyrene 34.51 252 3178753 11.17 ug/L 96 48) Indeno(l,2,3-cd)pyrene 37.33 276 1998554 10.53 ug/L 98 49) Dibenz(a,h)anthracene 37.45 278 2685574 12.87 ug/L 99 50) Benzo(g,h,i)perylene 38.06 276 2895908 13.07 ug/L 96
(#) = qualifier out of range (m) = manual integration (+) = signals summed REFl.D 052202.M Wed May 22 12:04:02 2002 Page 2
NYC-WTC_000013084
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NYC-WTC_000013913
GCMS calculation report for sample AE11602 dated May 30, 2002, listing concentrations of nitrosamines and chlorinated compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015524
Calibration verification data for volatile organic compound analysis using gas chromatography-mass spectrometry on June 5, 2002.
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Reference standard analysis report for volatile organic compounds using gas chromatography-mass spectrometry on June 5, 2002.
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Calculated reference values and recovery percentages for organic compound analysis using gas chromatography-mass spectrometry with all results at or above 2.0 ug reporting limit.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015373
Calibration verification data for volatile organic compound analysis using gas chromatography-mass spectrometry on June 10, 2002.
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GCMS calibration report for sample AE11602 dated May 30, 2002, showing quantitative results for volatile organic compounds.
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Laboratory report showing reference calculations for volatile organic compounds in sample AE12288 analyzed on June 3, 2002.
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Calibration data sheet verifying instrument response for volatile organic compounds during GCMS analysis on May 29, 2002.
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Laboratory report displaying calibration percentages for various volatile organic compounds including nitrosamines and chlorobenzenes.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024062
Laboratory report showing reference standard analysis results for nitrosamines and other compounds in sample AE10895.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023863
Calibration data for volatile organic compounds including nitrobenzene and isophorone from sample AE10901 analysis.
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Laboratory report documenting GCMS calibration verification for sample AE11410 conducted on May 22, 2002.
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NYC-WTC_000013043
DEP document containing gas chromatography-mass spectrometry data from May 2002.
Filed in the same folder
NYC-WTC_000013044
Fragmented header page from a GCMS document batch dated May 2002 showing Method 508.
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NYC-WTC_000013049
Laboratory report showing blank sample analysis for volatile organic compounds using gas chromatography-mass spectrometry on May 22, 2002.
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NYC-WTC_000013077
Laboratory report showing calibration analysis for volatile organic compounds using gas chromatography-mass spectrometry on May 22, 2002.
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NYC-WTC_000013089
GCMS laboratory report for sample AE09517 detecting unknown compounds and 2,4-DDD on May 23, 2002.
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