GCMS quantitative results for sample AE11602, May 2002

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Data File : C:\MSDCHEM\1\DATA\052802\524REF1.D Vial: 4 Acq On : 28 May 2002 4:45 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 30 10:35:49 2002 Quant Results File: 052202.RES 2.* Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 29 08:47:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 9.90 152 4727083 40.00 ug/L 0.00 10) Napthalene-d8 13.39 136 18984108 40.00 ug/L -0.02 17) Acenapthalene-dlO 18.53 164 10623690 40.00 ug/L -0.01 29) Phenanthranene-dlO 22.91 188 16118784 40.00 ug/L 0.00 37) Chrysene-dl2 30.76 240 11034134 40.00 ug/L -0.04 43) Perylene-dl2 34.66 264 6305118 40.00 ug/L -0.03 System Monitoring Compounds 27) TCMX 20.50 209 2338686 38.20 ug/L 0.00 Spiked Amount 40.000 Recovery 95.50% Target Compounds Qvalue 2) n-nitros-dimethyl amine 3.87 74 624113 7.07 ug/L # 80 3) bis(2-Chloroethyl)ether 9.31 93 2627313 15.00 ug/L 98 4) 1,3-Dichlorobenzene 9.73 146 2446421 13.87 ug/L 98 5) 1,4-Dichlorobenzene 9.94 146 2561123 13.36 ug/L 99 6) 1,2-Dichlorobenzene 10.32 146 2531144 15.00 ug/1 100 7) 2,2'oxybi s(1-Chioropropane 10.77 45 4260852m 15.88 ug/L 8) N-nitroso-di-propylamine 11.10 . 70 1798342 15.78 ug/L 97 9) Hexachloroethane 11.22 117 764977 11.01 ug/L 99 11) Nitrobenzene 11.45 77 2500596 15.00 ug/L 99 12) Isophorone 12.17 82 5391735 17.86 ug/L 99 13) bis(2-Chloroethoxy) methan 12.90 93 3329120 15.74 ug/L 99 14) 1,2,4-Trichlorobenzene 13.26 180 2103895 14.67 ug/L 100 15) Napthalene 13.45 128 8369126 16.72 ug/L 100 16) Hexachlorobutadiene 13.89 225 812121 11.86 ug/L 97 18) 2-Chloronaphthalene 16.89 162 4802978 17.65 ug/L 99 19) Dimethylphthalate 17.96 163 5518513 16.52 ug/L 99 20) 2,6-Dinitrotoluene 18.08 165 890013 16.59 ug/L 97 21) Acenapthylene 18.09 152 7352242 16.20 ug/L 99 22) Acenapthalene 18.62 153 4977685 17.37 ug/L 100 23) 2,4-Dinitrotoluene 19.23 165 1187637 16.93 ug/L 94 24) Diethylphthalate 20.10 149 5458311 17.49 ug/L 98 25) 4-Chlorophenyl-phenylether 20.29 204 2734022 16.42 ug/L 98 26) Fluorene 20.16 166 5973621 17.69 ug/L 99 28) Azobenzene 20.74 77 6012115 16.36 ug/L 99 30) Nnitrosodiphenylamine 20.65 169 3166143 19.47 ug/L 99 31) 4-Bromophenyl-phenylether 21.72 248 1396654 16.92 ug/L 97 32) Hexachlorobenzene 21.75 284 1414095 17.62 ug/L 99 3 3) Phenanthrene 22.97 178 8394615 17.32 ug/L 100 34) Anthracene 23.12 178 7568555 15.86 ug/L 99 35) Di-n-butylphthalate 25.05 149 8369584 17.38 ug/L 99 (#) = qualifier out of range (m) = manual integration 524REF1.D 052202.M Thu May 30 10:36:17 2002 Page 1

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