GCMS data file header for May 24-28, 2002

NYC 9/11 Public Portal Document ulDrary searen compouna Report

Data File : C:\MSDCHEM\1\DATA\052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ******************************************************************** * Peak Number 17 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 39.24 0.36 ug/L 190327 Perylene-dl2 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qua 1 3,6-Dioxa-2/4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0/40 2 2,6-Dimethyl-3,4-bis(trimethylsi... 311 C15H29NO2Si2 1000079-52-1 35 3 4H-Pyrido[l,2-a]pyrimidine-3-car... 221 C11H15N3O2 064399-29-/ 30 4 3,4-Bis-(methylthio)-quinoline 221 C11H11NS2 1000147-85-8 22 Abundance Scan 6155 (39.243 min): 524LB.D (-6142) (-) m/z 147.00 100.00% 1-17 221 73 5000 281

44 191 . 355 ..... All AMy f ‘ I * • ‘ * J ‘ ‘

m/z-> 0 '"I ““J"'i"1 TI’0013021000002307037 wl. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 39.00 39.20 39.40 39.60 m/z 221.00 86.26% Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,77... 147 21:1

5000 73

191 m/z / > rv 39.00 39.20 39.40 39.60 73.05 65.17%

A 117 279

mfz-> 0 28 45 *0000— 101 44 11754 [ 245263 | 295 ..fiii11....1....j.... 1.., 1.. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #87845:2,6-DimethyI-3,4-bis(trimethylsilyloxymethyl)pyridine 73 2211

39.00 39.20 39.40 39.60 5000 147 m/z 281.00 45.63%

178 _ 45 27 | .8 107131 194 1 266 298 01 TTTTTTTTamammT 1 IT’ IT rn I Iti I "I।(t j > D 11 11(1 1 n । 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #87940: 4H-Pyrido[1,2-alpyrimidine-3-carboxamide, 1,6,7,8-.. 211 39.00 39.20 39.40 39.60 m/z 207.00 32.46% 5000 whnakduyepo 81 109 135 162179 208 0 1’0"1’01111111110111’EEIE-1mmur "i ■ ■ “ i"" 11" 'i “ " 1" “ i‘ ■ ■ ■ i■ m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 39.00 39.20 39.40 39.60

524LB.D 052202.M Thu May 30 10:44:20 2002 Page 20

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