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GCMS analysis results sample AE12160, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12160 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000013405–000013413

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document LSC Area Percent Report . 'Data File : C:\HPCHEM\1\DATA\MAY2402\12160.D Vial: 14 Acq On : 25 May 2002 4:22 am Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.114 330 334 366 rBV 351762 950682 22.79% 4.280% 2 12.144 767 773 788 rBV 1203702 3050220 73.12% 13.731% 3 15.779 1163 1169 1187 rBV 2014762 4114025 98.62% 18.519% 4 21.086 1740 1747 1768 rBV 1950877 4171717 100.00% 18.779% 5 23.225 1971 1980 1988 rBV 885285 1796612 43.07% 8.088% 6 25.520 2223 2230 2242 rBV2 1886499 3843592 92.13% 17.302% 7 33.571 3101 3107 3127 rBV2 1036856 2428962 58.22% 10.934% 8 37.785 3558 3566 3580 rBV2 633770 1858865 44.56% 8.368%

Sum of corrected areas: 22214675 12160.D GCMS0520.M Tue May 28 12:05:19 2002

NYC-WTC_0000 13410

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NYC-WTC_000013410Source: NYC Law Department, mirrored locally

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