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GCMS analysis results sample AE12158, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12158 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000013387–000013395

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report : Data File : C:\HPCHEM\1\DATA\MAY2402\12158.D Vial: 12 Acq On : 25 May 2002 2:23 am Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.118 331 335 367 rVB 283060 797607 21.45% 4.003% 2 12.139 767 773 788 rBV 1031575 2716338 73.04% 13.632% 3 15.774 1163 1169 1187 rBV 1779594 3652354 98.21% 18.329% 4 21.081 1741 1747 1761 rBV 1830801 3718814 100.00% 18.662% 5 23.220 1972 1980 1988 rBV 787353 1601302 43.06% 8.036%

6 25.515 2224 2230 2242 rBV2 1569410 3412482 91.76% 17.125% 7 _ 33.575 3101 3108 3123 rBV2 982219 2257676 60.71% 11.330% 8 37.789 3559 3567 3582 rBV2 588452 1770193 47.60% 8.883%

Sum of corrected areas: 19926766 12158.D GCMS0520.M Tue May 28 12:05:00 2002

NYC-WTC_000013392

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NYC-WTC_000013392Source: NYC Law Department, mirrored locally

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