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GCMS analysis results sample AE12153, June 2002

Machine-extracted title · confidence 90%

Analytical report for sample AE12153 detailing GCMS results and surrogate recovery data from June 6, 2002.

NYC-WTC_000013342–000013350

Folder label: “GCMS X 5/22/02 A 5/25/02

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Scanned page image, NYC-WTC_000013347
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NYC 9/11 Public Portal Document

LSC Area Percent Report . Data File : C:\HPCHEM\l\DATA\MAY2402\12153 .D Vial: 7 Acq On : 24 May 2002 9:27 pm Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2"* Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) *es Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 8.115 330 334 362 rBV 320083 847062 21.29% 4.062% 2 12.136 767 772 793 rBV 1105098 2907466 73.08% 13.942% 3 15.772 1163 1168 1184 rBV 1809697 3881042 97.55% 18.611% 4 21.087 1740 1747 1763 rBV 1943071 3978366 100.00% 19.077% 5 23.226 1972 1980 1988 rBV 829473 1679160 42.21% 8.052% 6 25.521 2220 2230 2242 rBV2 1711363 3645523 91.63% 17.481% 7 33.572 3101 3107 3127 rBV2 957842 2225427 55.94% 10.671% 8 37.786 3558 3566 3582 rBV2 562390 1689900 42.48% 8.104%

Sum of corrected areas: 20853946 12153.D GCMS0520.M Tue May 28 12:04:10 2002

NYC-WTC_000013347

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NYC-WTC_000013347Source: NYC Law Department, mirrored locally

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