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GCMS analysis results sample AE12152, June 2002

Machine-extracted title · confidence 90%

Analytical report for sample AE12152 detailing GCMS results and surrogate recovery data from June 6, 2002.

NYC-WTC_000013333–000013341

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report * Data File : C:\HPCHEM\1\DATA\MAY2402\12152.D Vial: 6 Acq On : 24 May 2002 8:28 pm Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\T\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.121 331 335 364 rBV 303682 857568 21.33% 4.056% 2 12.142 767 773 790 rBV 1144222 2947821 73.31% 13.943% 3 15.777 1163 1169 1187 rBV 1919935 3926529 97.65% 18.572% 4 21.083 1740 1747 1761 rBV 1968806 4021180 100.00% 19.020% 5 23.222 1972 1980 1991 rBV 851040 17263'02 42.93% 8.165% 6 25.517 2224 2230 2241 rBV2 1713857 3657374 90.95% 17.299% 7 33.578 3101 3108 3129 rBV2 949801 2246609 55.87% 10.626% 8 37.782 3558 3566 3584 rBV2 602109 1758459 43.73% 8.317%

Sum of corrected areas: 21141842 12152.D GCMS0520.M Tue May 28 12:04:00 2002

NYC-WTC_000013338

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NYC-WTC_000013338Source: NYC Law Department, mirrored locally

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