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GCMS analysis results sample AE12160, June 2002

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Laboratory report documenting GCMS analysis of sample AE12160 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000013405–000013413

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data.File : C:\HPCHEM\1\DATA\MAY24O2\1216O. D Vial: 14 Acq On : 25 May 2002 4:22 am Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 12:02 2002 Quant Results File: >GCMS0520 .RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:39:13 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.14 152 562580 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 2229766 40.00 ug/1 -0.01 17) Acenaphthene-diO 21.09 164 1051028 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 1504964 40.00 ug/1 -0.01 38) Chrysene-dl2 33.57 240 765958 40.00 ug/1 -0.04 44) Perylene-dl2 37.78 264 500716 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.22 209 195173 36.95 ug/L 0.00 Spiked Amount 40.000 Recovery 92.38% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.42 74 187 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.15 146 694 N.D. 5) 1,4-Dichlorobenzene 12.15 146 694 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.83 128 248 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.57 149 335 N.D. 26) 4-Chlorophenylphenylether 23.22 204 1286 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.22 168 375 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.52 178 502 N.D. (#) = qualifier out of range (m) = manual integration 12160.D GCMS0520.M Tue May 28 12:03:05 2002 Page 1

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