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GCMS analysis results sample AE12160, June 2002

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Laboratory report documenting GCMS analysis of sample AE12160 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000013405–000013413

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY2402\12160.D Vial: 14 Acq On : 25 May 2002 4:22 am Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 12:02 2002 Quant Results File:'GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:39:13 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.52 178 502 N.D. 36) Di-n-butylphthalate 27.49 149 1813 N.D. 37) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.57 228 1719 N.D. 42) Bis(2-ethylhexyl)phthalate 33.80 149 721 N.D. 43) Chrysene 33.57 228 1719 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.79 252 2181 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 12160.D GCMS0520.M Tue May 28 12:03:06 2002 Page 2

NYC-WTC_000013408

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NYC-WTC_000013408Source: NYC Law Department, mirrored locally

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