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Document / 9 pages

GCMS analysis results sample AE12154, June 2002

Machine-extracted title · confidence 90%

Analytical report for sample AE12154 detailing GCMS results and surrogate recovery data from June 6, 2002.

NYC-WTC_000013351–000013359

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report •’ Data File : C:\HPCHEM\1\DATA\MAY2402\12154.D Vial: 8 Acq On : 24 May 2002 10:26 pm Operator: Morgan Sample : gc/ms scan 5/22 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P 2** xes Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.114 330 334 361 rBV 328606 818887 20.52% 3.874% 2 12.135 767 772 786 rBV 1126127 2879233 72.15% 13.621% 3 15.780 1163 1169 1186 rBV 1831938 3902646 97.80% 18.463% 4 21.086 1740 1747 1762 rBV 1885763 3990508 100.00% 18.879% 5 23.225 1971 1980 1988 rBV 792449 1620961 40.62% 7.669% 6 25.520 2223 2230 2241 rBV2 1758153 3721052 93.25% 17.604% 7 33.571 3101 3107 3127 rBV2 1041168 2343032 58.72% 11.085% 8 37.785 3558 3566 3590 rBV 630856 1861241 46.64% 8.805%

Sum of corrected areas: 21137560 12154.D GCMS0520.M Tue May 28 12:04:19 2002

NYC-WTC_000013356

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NYC-WTC_000013356Source: NYC Law Department, mirrored locally

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