GCMS calibration table data, sample AE09682, May 2002

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Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013277–000013284

Folder label: “GCMS X 5/21/02 A 5/21/02”

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B Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY0 602\9682.D Vial: 25 Acq On 7 May 2002 3:49 pm Operator: Sample GC/MS SCAN 4/25 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 9:26 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501 PN)

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.20 152 570951 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 2099761 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.13 164 1141433 40.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1582584 40.00 ug/1 -0.02 38) Chrysene-dl2 33.63 240 881686 40.00 ug/1 -0.04 44) Perylene-dl2 37.86 264 531275 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.27 209 33174 5.97 ug/L -0.03 Spiked Amount 10.000 Recovery = 59.70% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.89 128 396 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 950 N.D. 26) 4-Chiorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 3) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.58 178 266 N.D. (#) = qualifier out of range (m) = manual integration 9682.D GCMS0501.M Thu May 09 09:28:02 2002 Page 1

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GCMS calibration table data, sample AE09519, May 2002 · Box DEP Box 15

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Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

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