GCMS analysis report sample AE09517, May 23, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\9517.D Vial: 13 Acq On : 21 May 2002 11:07 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Ethanol, 2,2,2-trifluoro- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 4.70 0.45 ug/L 309189 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanol, 2,2,2-trifluoro- 100 C2H3F30 000075-89-8 / 2 2-Chloroethanol 80 C2H5C10 000107-07-yl 3 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 1 4 2-Chloroethanol 80 C2H5C10 000107-07-3 1 Abundance Scan 275 (4.695 min): 9517.D (-274) (-) m/z 49.10 100.00% 49 84

5000 42 58 35 4.40 4.60 4.80 5.00

n/z-> 01 mm-- 1 10 —..70—..8090 2030405060 IU 100 110 120 m/z 84.00 66.53% Abundance #108306: Ethanol, 2,2,2-trifluoro- 31

5000 ■ • ■ 11 • ■ ■ ■ । • ■ ■11 • ■ ■ ■ i ■ ■ ■ ■ 4.40 4.60 4.80 5.00 m/z 48.10 43.89% 69 8151 61 miz-> 0 11111111125. 10 20 +44 301 40 LL 50 60 99 ■ I' ‘ ■ ''r''1 * * । * । ■ * । > * ■ * । <' * < । < * 70 80. 90 100 110 120 Abundance #108291:2-Chloroethanol 31 ■ ■ ■ i ' 1 ‘ ' i • ' • • i ■ ■ ■ ■ i ■ ■ ■ • 4.40 4.60 4.80 5.00 5000 m/z 50.05 32.06%

0 — Lll 15 43 49 80 721 ■ i11 > 'T-- 11111**1*741/11 JMYAurospmbs miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1082: Ethanol, 2,2-dichloro- ■ ■ i ■ ■ ■ ■ i ■ ■ 31 4.40 ’ 4.60 4.80 5.00 m/z 42.001 23.45%

5000

0 25., 37 43 49 55 61 70 77, 83 96 103 114 1 1111 ■1 r1' •' r1'1 * < । * • i 11.. 111. i.. ।. >,, ।1111,, m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 4.40 4.60 4.80 5.00

9517.D 052202.M Wed May 22 11:29:27 2002 Page 14

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