GCMS sample analysis results, AE11906, June 3, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11906.D Vial: 13 Acq On : 22 May 2002 11:36 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 l-Buten-3-yne, 2-chloro­ Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.81 1.16 ug/L 904161 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Buten-3-yne, 2-chloro- 86 C4H3C1 017712-36/6 7 2 Ethanamine, N-ethyl-N-[(ethylthi... 147 C7H17NS 003492-79-3 4 3 Ethanamine, N-(ethoxymethyl)-N-e ... 131 C7H17NO 007352-/3-6 4 4 5-Fluoroimidazole 86 C3H3FN2 . 1000128-06-0 2

./"Mu, Abundance Scan 124 (3.808 min): 11906.D (-122) (-) m/z 35.10 100.00% 35

42 4 MM 86 5000

, 49 RR

0-r I| 1.58........ 3.40 3.60 3.80 4.00 4.20 i ■ •1 ■ । ‘ । ■ ■ • ■ i ■ ■ ■ ■ i ■ • • 1 । m/z 42.10 60.00% miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #34744:1-Buten-3-yne, 2-chloro- 51 86

5000 1**‘*I****1*1** 3.40 3.60 3.80 4.00 4.20 m/z 86.00 50.99% 60 0— 11 ! I I | I I I I | I I I I | > I T miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #34671: Ethanamine, N-ethyl-N-[(ethylthio)methyl]- 86 3.40 3.60 3.80 4.00 4.20 5000 m/z 88.00 50.33% 42 58 47 70 75 O', u ■ ■ ■ ■ i 1ul TIid I I j___________ ________________________________ trer (11 ■ i • ■ ■ 1 i ■ ' • ■ i ■ ■ ■ ■ i ■ 1 • ‘ i ■ ■ ■ ■ i miz-> 30 40 50 60 701 80 90 100 110 120 130 Abundance #3590: Ethanamine, N-(ethoxymethy!)-N-ethyl- 42 3.40 3.60 3.80 4.00 4.20 m/z 43.10 30.11% 5000- 86 70 56

m/z-> 0 ■ p 30 40 I X 1 I 1 I I ' I < < 1 I I I 50 60 70 1-12 ' ‘ i 1 1 80 90 100 110 116 120 131 130 ■ 1 1 i ■ ■ ■ ■ i'1 ■ ■ ■ i

3.40 3.60 3.80 4.00 4.20

11906.D 052202.M Tue May 28 12:13:08 2002 Page 6

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