GCMS sample AE12765 results, June 6 2002

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Gas chromatography-mass spectrometry analysis report for sample AE12765 detecting unknown compounds and surrogates on June 6, 2002.

NYC-WTC_000015536–000015560

Folder label: “GCMS X 6/4/02 A 6/4/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \MSDCHEM\1\DATA\060402\12765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 l-Buten-3-yne, 1-chloro-, (Z)- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.03 2.31 ug/L 1486540 1,4-dichlorobenzene-d4 9.90 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l l-Buten-3-yne, 1-chloro-, (Z)- 86 C4H3C1 020374-90-7 4 2 l-Buten-3-yne, 1-chloro-, (Z)- 86 C4H3C1 020374-90-7/7 3 1,2,3-Butatriene, 1-chloro- 86 C4H3C1 020658-21-3 7 4 l-Buten-3-yne, 1-chloro-, (E)- 86 C4H3C1 020374-91-8 7 Abundance Scan 162 (4.031 min): 12765.D (-160) (-) m/z 51.10 '00.00%| 51 85

35 48 5000

42 3.60 3.80 4.00 4.20 4.40 [

niz-> 15 oh 1111’4’1’144114 20 25 30 JXu 35 40 45 50 55 60 65 70 75 82 [ 80 85 ■ i' ■ ■ ■ i ■ ■ 90 95 m/z 86.00 100.00% Abundance #111070: 1-Buten-3-yne, 1-chloro-, (Z)- 51 86

5000 i ■ ■ ■ ■ i ‘ ■ i ■ ■ 1 1 i ' 1 1 1 1 1 1 3.60 3.80 4.00 4.20 4.40 m/ z 86.90 66.67%

4wyhe 60 0— ■ ■ i ■ " ' i ■ " ■ i1 “ ■ i " '11 “111" ' ’ I' '1111111111" 11111111 " 11" 11 m ' l ' niz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12406:1-Buten-3-yne, 1-chloro-, (Z)- A 51 86 .4,717711/11/1III 3.60 3.80 4.00 4.20 4.40 5000

0 26 30 37 43 48 i 1 I 1 I I 1 I I r> I I I n-1 | 1 I 11 I I I I 1 | | ! I I +6063, . 7174111/83+ 1 “ i “ “ 1 ■1 ■ • 1 ■ 39 TTTTITT m/z

Mysss.. 35.10 57.04%

/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #12404:1,2,3-Butatriene, 1-chloro- 51 86 3.60 3.80 4.00 4.20 4.40 | m/z 48.10 56.54% 5000

39 O- 1 ■ i" “ । ■"111 r“ i" “ i “ “ i1111 . “ i “ “60 111 “ i'1 “ i11'11" " i1"' 1 T' i1 “ 1111 n/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20 4.40

12765.D 060302.M Wed Jun 05 14:05:29 2002 Page 10

NYC-WTC_000015550

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