GCMS sample analysis results, AE11800, June 3, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11800.D Vial: 7 Acq On : 22 May 2002 6:43 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e g*.* Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Tetraborane(10) Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 3.82 0.89 ug/L 606264 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Te t raborane(10) 54 B4H10 018283-93-7 10 2 Propiolonitrile 51 C3HN 001070-71-93 3 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 2 4 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 2 Abundance Scan 127 (3.826 min): 11800.D (-125) (-) m/z 84.00 100.00% 51 84 43 5000 35 3.40 3.60 3.80 4.00 4.20 m/z 51.10 77.51%

_/Ww 0- ‘ ■ i • • ■ ■ i 1 ■ ■ ■ i ■ • miz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #12315: Tetraborane(10) 48

5000 ■ । ‘ । ■ • • ■ । ■ • • ■ ।1 ‘ 1 11 ■ ■1 35 3.40 3.60 3.80 4.00 4.20 11 m/z 48.10 64.21%

miz—> 0-

Abundance 0 I -pl24 , 10 +2 20 30 40 50 60 70 80 #12371: Propiolonitrile 51 90 100 110 120 wWMr 1***’I*’’’I**’*1***I*** 3.40 3.60 3.80 4.00 4.20 5000 m/z 43.10 53.58%

12 . 25 38 "nppn#“MMMaly 0- mHi 18,12 I ' ■ ■ i ' ■ ' ■ i ' ■ ■ ■ i • ■ ■ ■ i ■ ■ ■ ■ i ‘ ‘ ■ i ' ■ ■ ■ i ■ ■

iz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1082: Ethanol, 2,2-dichloro- 31 3.40 3.60 3.80 4.00 4.20 m/z 50.10 42.13% 5000

37 43 49 55 61 70 77, 83 96 103 —114 wMw 0- ■ ■ I 1 1 ■ ■ I ' 25 , 1*11p****mmu ' 1’1t e n/z-> 0 10 20 301 40 50 60 70 80 90 100 110 120 3.40 3.60 3.80 4.00 4.20

11800.D 052202.M Tue May 28 12:04:26 2002 Page 6

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