NYC 9/11 Public Portal Document
yUdt-tata’L RSPUL L 11 KEVLEwtu/
Data-File : C:\MSDCHEM\l\DATA\052902\LBB0529.D Vial: 15
Acq On : 29 May 2002 1:53 pm Operator: Bohlk / Inst 213
* Sample : LB 5/23/02 Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: rteint.p
Quant Time: Jun 03 15:45:28 2002 Quant Results Files 052802.RES
Quant Method : C:\MSDCHEM\l\5973N\052802.M (RTE Integrator) 2**
Title : Quantitation For Method 525.2
Last Update : Mon Jun 03 15:34:22 2002
Response via : Initial Calibration
DataAcq Meth : 052802
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 18.19 164 1877139 5.00 ug/L 0.00
9) Phenanthrene d-10 22.51 188 2876960 5.00 ug/L 0.00
19) Chrysene d-12 30.29 240 1921021 5.00 ug/L 0.00
25) p-Terphenyl d-14 27.39 244 2249221 5.00 ug/L 0.00
System Monitoring Compounds
2) l,3-Dimethyl-2-nitrobenzen 13.11 134 521732 4.95 ug/L 0.00
Spiked Amount 5.000 Recovery = 99.00%
20) Triphenyl Phosphate 29.57 326 414683 5.08 ug/L 0.00
Spiked Amount 5.000 Recovery = 101.60%
21) Perylene D-12 34.30 264 935023 3.65 ug/L 0.00
Spiked Amount 5.000 Recovery = 73.00%
26) Acenaphthene d-10 (surr) 18.19 164 1877139 3.75 ug/L 0.00
Spiked Amount 5.000 Recovery = 75.00%
27) Phenanthrene d-10 (surr) 22.51 188 2876960 4.12 ug/L 0.00
Spiked Amount 5.000 Recovery = 82.40%
28) Chrysene d-12 (surr) 30.29 240 1921021 4.20 ug/L 0.00
Spiked Amount 5.000 Recovery = 84.00%
Target Compounds Qvalue
3) Hexachlorocyclopentadiene 0.00 237 0 N.D.
4) Hexachlorobenzene 0.00 284 0 N.D.
5) EPTC 0.00 128 0 N.D.
6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
7) 2,4-Dinitotoluene 0.00 165 0 N.D.
8) Molinate 0.00 126 0 N.D.
10) Simazine 0.00 201 0 N.D.
11) Atrazine 0.00 200 0 N.D.
12) Alachlor 0.00 160 0 N.D.
13) Terbacil 0.00 117 0 N.D.
14) Acetochlor 0.00 146 0 N.D.
15) Metribuzin 0.00 198 0 N.D.
16) Metolachlor 0.00 162 0 N.D.
17) Butachlor 0.00 160 0 N.D. d
18) 4,4’-DDE 0.00 246 0 N.D. d
22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. d
23) Bis (2-Ethylhexyl) phthala 30.95 149 67250 0.84 ug/L 96
24) Benzo (a) pyrene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBB0529.D 052802.M Mon Jun 03 15:46:22 2002 Page 1
NYC-WTC_000012566
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