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GCMS calibration data for Method 508, Mar 6 2002

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Calibration table and chromatographic data for GC/MS analysis using Method 508 conducted on March 6, 2002.

NYC-WTC_000011575–000011582

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\MAR0102\3437.D Vial: 49 Acq On 3 Mar 2002 11:35 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 6 11:43 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Mar 06 11:41:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.72 178 753 N.D. 34) Anthracene 25.72 178 753 N.D. 35) Di-n-butylphthalate 27.68 149 1118 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.79 228 3596 N.D. 42) Bis(2-ethylhexyl)phthalate 33.99 149 3986 N.D. 43) Chrysene 33.79 228 3596 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.07 252 3914 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 3437.D GCMS0208.M Mon Mar 25 12:14:39 2002 Page 2

NYC-WTC_000011576

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NYC-WTC_000011576Source: NYC Law Department, mirrored locally

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