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← Document results/DEP Box 14/GCMS X 2/14/02 A 3/2/02 - 3/20/02
Document / 8 pages

GCMS calibration table for TCLP method, March 2002

Machine-extracted title · confidence 100%

Instrument output displaying calibration data and surrogate recovery results for sample AE03380.

NYC-WTC_000011477–000011484

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011480
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

"Data File C:\HPCHEM\1\DATA\MAR0102\3380.D Vial: 44 Acq On 3 Mar 2002 6:37 am Operator: Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.185 338 342 359 rBV 117482 334983 5.40% 1.113% 2 12.316 786 792 811 rBV 1802224 4397628 70.91% 14.608% 3 15.961 1182 1189 1206 rBV 2590948 5872569 94.69% 19.508% 4 21.276 1761 1768 1786 rBV 2686349 6201792 100.00% 20.601% 5 25.729 2245 2253 2263 rBV2 2585755 6079882 98.03% 20.196%

6 25.857 2263 2267 2278 rVB 30417 96320 1.55% 0.320% 7 30.796 2799 2805 2810 rBV 136066 292124 4.71% 0.970% 8 33.789 3123 3131 3149 rBV2 1513098 3871928 62.43% 12.862% 9 38.067 3587 3597 3624 rBV2 876827 2956600 47.67% 9.821%

Sum of corrected areas: 30103826

3380.D GCMS0208.M Mon Mar 25 12:19:47 2002

NYC-WTC_000011480

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NYC-WTC_000011480Source: NYC Law Department, mirrored locally

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