GCMS reference analysis results for sample AE03265, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\031902\0214REF1.D Vial: 31 Acq On : 20 Mar 2002 5:04 pm Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 25 08:58:58 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cop- Units Dev(Min)

9.54 1437444 ,/20.00 ug/L 1) 1,4-Dichlorobenzene-d4 150 0.00 10) Naphthalene-d8 13.03 136 3766395 20.00 ug/L 0.00 17) 29) 38) Acenaphthene-diO Phenanthrene-diO Chrysene-dl2 18.13 22.50 30.31 164 188 240 2092802 3231212 2973434 20.00 ug/L 20.00 ug/L 20.00 ug/L 0.00 0.00 0.00 6 44) Perylene-dl2 34.18 264 1665851 20.00 ug/L 0.00 lo System Monitoring Compounds 37) 2,4-ddd surr Spiked Amount 5.000 27.43 235 287143 Recovery 7.45 ug/L = 149.00% 0.00 b' 0 Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.59 74 164288 5.09 ug/L 100 3) bis(2-chloroethyl) ether 8.98 93 519304 10.21 ug/L 83 4) 1,3 - Dichlorobenze 9.38 146 386014 7.67 ug/L 97 5) 1,4 - Dichlorobenzene 9.59 146 397283 7.92 ug/L 99 6) 1,2 - Dichlorobenzene 9.96 146 413214 8.89 ug/L 98 7) 2,2 1 - oxybis (l-Chloropr 10.42 45 1230390 10.62 ug/L 100 8) N-Nitroso-di-n-propylamine 10.75 70 428824 11.72 ug/L 95 9) Hexachloroethane 10.86 117 125708 6.67 ug/L 99 11) Nitrobenzene 11.10 77 546002 8.05 ug/L 98 12) Isophorone 11.81 82 1219199 9.77 ug/L 99 13) bis(2-Chloroethoxy) methan 12.55 93 661768 8.81 ug/L 99 14) 1,2,4-Trichlorobenzene 12.90 180 338678 7.85 ug/L 99 15) Naphthalene 13.08 128 1483460 9.48 ug/L 99 16) Hexachlorobutadiene 13.53 225 131949 5.47 ug/L 96 18) Hexachlorocyclopentadiene 15.61 237 13637 0.74 ug/L 90 19) 2-chloronaphthalene 16.51 162 915936 9.59 ug/L 98 20) Dimethylphthalate 17.59 163 1253377 10.99 ug/L 98 21) 2,6-Dinitrotoluene 17.70 165 224479 9.25 ug/L 94 22) Acenaphthylene 17.70 152 1346028 10.16 ug/L 99 2 3) Acenaphthene 18.22 153 931098 10.33 ug/L 99 24) 2,4-Dinitrotoluene 18.86 165 288142 8.29 ug/L 96 25) Diethylphthalate 19.72 149 1153458 11.75 ug/L 99 26) 4-Chlorophenyl-phenyl ethe 19.89 204 560294 10.71 ug/L 97 27) Fluorene 19.76 166 1217364 11.46 ug/L 100 28) Azobenzen/ 1,2-Diphenylhyd 20.35 77 1438830 9.94 ug/L 95 30) N-Nitrosodiphenylamine 20.26 169 496475 7.15 ug/L 99 31) 4-Bromophenyl-phenyl ether 21.32 248 327456 11.48 ug/L 94 32) Hexachlorobenzene 21.34 284 344753 11.46 ug/L 97 3 3) Phenanthrene 22.56 178 1727376 11.54 ug/L 99 34) Anthracene 22.70 178 1534369 10.33 ug/L 100 35) Di-n-butylphthalate 24.64 149 2066932 12.05 ug/L 99 3 6) Fluoranthene 26.06 202 2019295 11.87 ug/L 99 39) Pyrene 26.69 202 2127982 10.35 ug/L 98 40) Butylbenzylphthalate 29.05 149 825045 9.37 ug/L 99 41) Benzo (a) antracene 30.29 228 1656163 10.61 ug/L 99 42) Bis (2-ethylhexyl) phthala 30.91 149 1178384 10.13 ug/L 100 43) Chrysene 30.38 228 1760986 11.88 ug/L 99 45) Di-n-Octylphthalate 32.75 149 1650261 9.22 ug/L 98 46) Benzo (b) fluoranthene 33.23 252 1301462 11.09 ug/L 100

(#) = qualifier out of range (m) = manual integration 0214REF1.D 5080302.M Mon Mar 25 08:59:55 2002 Page 1

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