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GCMS analysis results for sample AE03075, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010947–000010966

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' * Data. File : C:\MSDCHEM\l\5973N\02FEB28\02717.D Vial: 2 Acq On : 28 Feb 2002 3:30 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\METH0DS\METHQDS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.611 19 21 27 rBV 35421 56700 0.47% 0.091% 2 3.916 45 48 53 rBV 19708 27400 0.23% 0.044% 3 3.995 53 55 61 rBV4 4811 17400 0.15% 0.028% 4 4.243 75 77 85 rW5 6332 17474 0.15% 0.028% 5 5.936 223 227 239 rBV 42412 126559 1.06% 0.203%

6 6.117 239 243 259 rVB4 7073 29490 0.25% 0.047% 7 9.707 557 561 575 rW 3474180 7318692 61.25% 11.732% 8 9.888 575 577 595 rVB4 4093 30498 0.26% 0.049% 9 12.540 807 812 815 rBV 8357 17488 0.15% 0.028% 10 13.195 865 870 875 rBV 5381935 10476656 87.67% 16.794% 11 13.376 885 886 893 rVB 11694 20438 0.17% 0.033% 12 16.548 1163 1167 1171 rBV 9819 18866 0.16% 0.030% 13 18.332 1319 1325 1331 rBV 5425195 11175695 93.52% 17.914% 14 22.283 1671 1675 1681 rW 29875 62034 0.52% 0.099% 15 22.633 1701 1706 1711 rBV2 5475567 11949554 100.00% 19.155% 16 24.857 1899 1903 1915 rW 16816 38545 0.32% 0.062% 17 27.724 2153 2157 2163 rBV 792984 1374894 11.51% 2.204% 18 30.490 2397 2402 2439 rBV2 4604381 11147243 93.29% 17.869% 19 31.099 2451 2456 2461 rVB2 12079 23756 0.20% 0.038% 20 34.407 2743 2749 2781 rBV 2895021 8455471 70.76% 13.554%

Sum of corrected areas: 62384853

02717.D HP022102.M Fri Mar 01 10:07:20 2002 Page 1

NYC-WTC_000010951

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