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GCMS analysis report for sample AE01510, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010027–000010046

Folder label: “GCMS X 1/23/02 A 2/21/02”

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Scanned page image, NYC-WTC_000010030
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NYC 9/11 Public Portal Document LSC Area Percent Report . • Data File : C:\MSDCHEM\1\5973N\02FEB21\01510.D Vial: 5 Acq On : 21 Feb 2002 2:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 3.498 7 1 9 11 19 rVB 25816 42630 0.28% 0.053% 2 3.622 19 22 29 rVB 44340 70261 0.46% 0.087% 3 3.927 47 49 55 rVB 22984 37728 0.24% 0.047% 4 4.378 85 89 95 rVB 21246 32697 0.21% 0.041% 5 5.948 225 228 237 rBV2 64643 240299 1.56% 0.298% 6 6.060 237 238 255 rVB 69730 227971 1.48% 0.283% 7 9.718 557 562 567 rBV 5026342 9133219 59.16% 11.323% 8 9.876 573 576 593 rVB 15818 77760 0.50% 0.096% 9 13.195 865 870 875 rBV 7049848 13611437 88.16% 16.876% 10 13.376 883 886 893 rVB2 14432 32628 0.21% 0.040% 11 18.343/1321 1326 1331 rBV 7332585 14701118 95.22% 18.227% 12 19.980//1467 1471 1481 rVB3 17562 51884 0.34% 0.064% 13 22.283/ 1671 1675 1683 rVB 48329 98114 0.64% 0.122% 14 22.644 /1701 1707 1711 rBV 7004077 15439152 100.00% 19.142% 15 22.768/ 1715 1718 1741 rVB 103193 529173 3.43% 0.656% 16 24.856 1899 1903 1909 rBV 15906 33952 0.22% 0.042% 17 27.724 2153 2157 2163 rW 1036914 1888779 12.23% 2.342% 18 30.490 2397 2402 2441 rBV2 5589942 13744739 89.03% 17.041% 19 33.402' 2655 2660 2665 rBV2 45364 100968 0.65% 0.125% 20 34.418 2743 2750 2779 rBV 3640342 10563245 68.42% 13.096%

Sum of corrected areas: 80657754

01510.D HP022102.M Mon Feb 25 10:55:08 2002 Page 1

NYC-WTC_000010030

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NYC-WTC_000010030Source: NYC Law Department, mirrored locally

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