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GCMS analysis report for sample AE01636, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010086–000010105

Folder label: “GCMS X 1/23/02 A 2/21/02”

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Scanned page image, NYC-WTC_000010090
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02FEB21\01636.D Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.622/ 19 22 31 rBV 40935 72502 0.50% 0.100% 2 3.927/ 47 49 57 rVB 19350 36632 0.25% 0.050% 3 4.266/ 75 79 87 rW2 12446 33663 0.23% 0.046% 4 4.379/ 87 89 93 rVB2 13241 24213 0.17% 0.033% 5 5.033/ 143 147 153 rVB2 11253 26035 0.18% 0.036%

6 5.948/ 223 228 245 rW 45957 154455 1.07% 0.212% 7 6.185V 245 249 263 rW3 4225 21784 0.15% 0.030% 8 9.718 557 562 567 rBV 4470786 8561273 59.29% 11.760% 9 9.899/ 575 578 591 rVB5 6397 31951 0.22% 0.044% 10 13.195 865 870 875 rBV 6628290 12632869 87.49% 17.353%

11 13.376/ 883 886 895 rVB312538 31151 0.22% 0.043% 12 16.548/ 1163 1167 1171 rVB11220 19549 0.14% 0.027% 13 18.332 1321 1325 1331 rBV 6505362 13761323 95.31% 18.903% 14 19.9801,1467 1471 1479 rVB3 7746 22364 0.15% 0.031% 15 22.283V 1671 1675 1685 rVB 35402 84231 0.58% 0.116%

16 22.633 1701 1706 1711 rBV2 6336014 14438537 100.00% 19.833% 17 24.857V 1899 1903 1915 rW 11475 31105 0.22% 0.043% 18 27.724 2153 2157 2163 rBV 846890 1489229 10.31% 2.046% 19 30.490 2397 2402 2437 rBV2 5095813 12378150 85.73% 17.003% 20 34.407 2743 2749 2779 rBV 3145531 8948542 61.98% 12.292%

Sum of corrected areas: 72799558

01636.D HP022102.M Mon Feb 25 10:55:36 2002 Page 1

NYC-WTC_000010090

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NYC-WTC_000010090Source: NYC Law Department, mirrored locally

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