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GCMS analysis results, sample AE02719, March 2002

Machine-extracted title · confidence 68%

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

NYC-WTC_000010987–000011006

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report ‘ ’ Data File : C:\MSDCHEM\l\5973N\02FEB28\02719.D Vial: 4 Acq On : 28 Feb 2002 5:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.622 19 22 29 rVB 32172 53835 0.46% 0.090% 2 3.927 45 49 51 rBV 21628 28523 0.24% 0.047% 3 3.995 51 55 61 rVB2 6343 23915 0.20% 0.040% 4 4.254 73 78 85 rVB5 12768 36073 0.31% 0.060% 5 4.379 85 89 93 rBV2 8046 15485 0.13% 0.026% 6 4.898 133 135 143 rBV2 5135 14499 0.12% 0.024% 7 5.936 223 227 243 rBV 50976 138801 1.18% 0.231% 8 9.707 557 561 567 rBV 3576375 7075874 60.32% 11.783% 9 9.888 573 577 581 rBV2 4052 13348 0.11% 0.022% 10 13.195 865 870 875 rBV 5263400 10150581 86.53% 16.903% 11 13.376 883 886 901 rVB 9216 33466 0.29% 0.056% 12 16.548 1163 1167 1171 rW 9033 16104 0.14% 0.027% 13 18.332 1319 1325 1331 rBV 5427431 10936651 93.23% 18.212% 14 22.283 1671 1675 1681 rVB 31314 58931 0.50% 0.098% 15 22.633 1701 1706 1711 rBV2 5373333 11730536 100.00% 19.535% 16 23.231 1755 1759 1765 rVB3 3894 14155 0.12% 0.024% 17 24.857 1899 1903 1911 rBV 18851 46894 0.40% 0.078% 18 27.724 2153 2157 2163 rW 639162 1114859 9.50% 1.857% 19 30.490 2397 2402 2439 rBV 4450959 10641188 90.71% 17.720% 20 34.407 2743 2749 2791 rBV 2753370 7906570 67.40% 13.167%

Sum of corrected areas: 60050288

02719.D HP022102.M Fri Mar 01 10:07:33 2002 Page 1

NYC-WTC_000010991

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