GCMS blank analysis report for sample AE02713, March 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report ’ Data File : C:\MSDCHEM\1\5973N\02FEB28\0205B.D Vial: 1 Acq On : 28 Feb 2002 10:30 am Operator: Sample : lab blank 2/5 Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 2-phenyl-.beta.-carbboline .. Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 29.68 0.02 ug/L 13284 Chrys ene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-phenyl-.beta.-carbboline $$ 9H... 244 C17H12N2 091944-01-3 8 7! 21,2-DICYANO-1,2-DIPHENYLCYCLOPRO...244C17H12N2 000000-00-0 7 3 (5-(2)H)1,3-DIMETHYL-(5,10-DIHYD... 244 C13H12DN3O2 000000-00-0 7 4 1-Pyrenecarboxaldehyde hydrazone 244 C17H12N2 076465-53-7 5 Abundance Scan 2330 (29.677 min): 0205B.D (-) m/z 244.10 100.00% 244

50001 122 ■ 1 i ‘ ■ i i ■ ■ ■ ■ i ' ■ 207 29.40 29.60 29.80 30.00 0' m/z 243.00 61.21% niz-> 60 80 100 120 140 160 180 200 220 240 Abundance #179478:2-pheny)-.beta.-carbboline $$ 9H-Pyrido[3,4-b]ind... 2-4

5000 ■ ■ i ■ ■ ■ ■ i ■ ■ 1 i 1 1 ■ ■ i ■ ■ 29.40 29.60 29.80 30.00 m/z 122.00 35.45% 122 0- • • i • ■ ■ ' i • ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ‘ • i ■ ■ • • i ' ■ ■ ■ i ■ ■ ■ 1 i ■ ■ ■ • i ■ ■ ■ ■ i '

n/z-> 60 80 100 120 140 160 180 200 220 240 Abundance #179472:1.2-DICYANO-1,2-DIPHENYLCYCLOPROPANE 244 166 217 29.40 29.60 29.80 30.00 5000 m/z 245.10 34.12% 140 51 Y 88 189 203 114 177 || || 0- 1 1 । 1 TO—RGmOmTmMTT 1 ' 1 • 1 i ■ ‘ TIM’ITII i • ■ ■ ■ i n/z-> 60 80 100 120 140 160 180 200 220 240 Abundance #177542: (5-(2)H)1,3-DIMETHYL-(5,10-DlHYDRO)-5-DEAZA-ALLOX... * 1 i • T T 244 29.40 29.60 29.80 30.00 m/z 207.00 13.92% 129 5000 186 229 Y 158

iz-> 0 • ■ i > • 60 • ■ i

80 ■ ■ ■ ‘

100 i ■ 1 ■ '

120 i ■ .2 ‘ ‘ i 140 200 ' ' ' ‘ i ■ ‘ 1 ‘ i ■ ■ ■ ' i ' 160 180 213 - • ‘ I1 1 220 240 ■ • i

29.40 29.60 29.80 30.00

0205B.D HP022102.M Fri Mar 01 10:06:47 2002 Page 15

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