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Document / 7 pages

GCMS calibration table results, February 27-March 19, 2002

Machine-extracted title · confidence 70%

Gas chromatography-mass spectrometry calibration analysis with retention times and response values for PAH standards and 2,4-DDD compound detection.

NYC-WTC_000010421–000010427

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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Scanned page image, NYC-WTC_000010424
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB2502\1964.D Vial: 36 Acq On : 27 Feb 2002 12:26 am Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.198 341 344 352 rBV 11150 24671 1.01% 0.205% 2 12.320 787 793 808 rVB 737269 1727642 70.58% 14.356% 3 15.955 1183 1189 1207 rBV 1074301 2287313 93.44% 19.007% 4 21.271 1761 1768 1783 rBV 1164343 2447930 100.00% 20.342% 5 25.714 2245 2252 2263 rBV2 1040890 2288926 93.50% 19.020%

6 30.791 2800 2805 2813 rVB 122345 235818 9.63% 1.960% 7 33.784 3124 3131 3148 rBV 752106 1705769 69.68% 14.174% 8 38.052 3588 3596 3612 rBV2 423515 1316093 53.76% 10.936%

Sum of corrected areas: 12034162

1964.D GCMS0208.M Tue Mar 19 11:02:13 2002

NYC-WTC_000010424

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NYC-WTC_000010424Source: NYC Law Department, mirrored locally

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