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Document / 6 pages

GCMS calibration table for TCLP analysis, February-March 2002

Machine-extracted title · confidence 95%

Calibration data file listing retention times and response factors for standard compounds used in TCLP testing procedures.

NYC-WTC_000010397–000010402

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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Scanned page image, NYC-WTC_000010400
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB2502\1960.D Vial: 32 Acq On : 26 Feb 2002 8:29 pm Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.320 787 793 805 rVB 581175 1484878 71.08% 14.702% 2 15.956 1183 1189 1207 rBV 920779 1963694 93.99% 19.443% 3 21.271 1761 1768 1779 rBV 974904 2089161 100.00% 20.686% 4 25.714 2246 2252 2264 rBV2 872489 1907239 91.29% 18.884% 5 30.791 2800 2805 2812 rVB 91414 179740 8.60% 1.780%

6 33.784 3124 3131 3144 rBV2 584980 1395957 66.82% 13.822% 7 38.053 3588 3596 3609 rBV2 358288 1078967 51.65% 10.683%

Sum of corrected areas: 10099636

1960.D GCMS0208.M Tue Mar 19 11:00:25 2002

NYC-WTC_000010400

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NYC-WTC_000010400Source: NYC Law Department, mirrored locally

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