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GCMS analysis results for sample AE01650, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01650 conducted on March 4, 2002, including surrogate recovery data.

NYC-WTC_000010176–000010186

Folder label: “GCMS X 1/25/02 A 2/25/02

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Scanned page image, NYC-WTC_000010183
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2 502\1650.D Vial: 6 Acq On : 25 Feb 2002 4:26 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 Pentane, 3-methoxy- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.36 ug/1 25656 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 1-But anamine, 3-methyl- 87 C5H13N 000107-85-7 4 4 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 4 Abundance / Scan 344 (8.203 min): 1650.D (-) i m/z 73.00... 100.00% 73

5000 43

, 87 207 7.80 ..— - 8.00 8.20 8.40 8.60 ii * * | > I l'l | . . I I j l < > I | > l . . J . . I I | . i i , > i i > j i i ■ i | i u . | i H I | I l I 1 | < i < < | 1 I |...,|....| . TTi . | . M | 1 i"“i‘ | ■ m/ Z 27.90% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1793: Pentane, 3-methoxy- 73

/ 5000 45 । 7.80 8.00 8.20 8.40 8.60 m/ z 40.95 12.11% 27 55 TT— (> ■ "i TH 1′1171111119112113111171101111191171111101111111111/22/1117211 m/Z? 10 20 30 40 50 60-70 80 90 100110 120 130.140 150 160170180190200210 Abundance 30 73 +7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 10.04% 44 58 15 l"*'l I.... I.... I i I.. I < 1111.... I >>>>!>>>. I.... 1 .>.>] 111 (1111! 1111J11111 (111T" 11 ■' ] 1111! 1111 ] 1111 (111 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #763: 1-Butanamine,3-methyl-..... . ■ i ■ ■ ■ ‘ i ■ ■ ■ ■ i ■ 1 ' ■ I ■ ■ ■ ■ i ■ • 30 7.80 8.00 8.20 8.40 8.60 m/ z 70.90 6.92% 5000

......... 15 4155 ...... 7.80 8.00 8.20 8.40 8.60 j m/z~> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210

1650.D GCMS0208.M Thu Feb 28 09:30:02 2002 Page 1

NYC-WTC_000010183

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NYC-WTC_000010183Source: NYC Law Department, mirrored locally

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