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GCMS analysis results for sample AE01638, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010126–000010145

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document LSC Area Percent Report . .Data File : C:\MSDCHEM\1\5973N\02FEB21\01638.D Vial: 7 Acq Ori : 21 Feb 2002 8:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.622/ 19 22 25 rBV 48272 68835 0.41% 0.078% 2 3.938% 47 50 57 rVB 23272 47865 0.29% 0.054% 3 4.379% 87 89 93 rVB 16482 29436 0.18% 0.034% 4 5.948* 223 228 249 rVB 61212 196879 1.18% 0.224% 5 9.718 557 562 567 rBV 5029062 10048575 60.02% 11.441% 6 9.887J 573 577 593 rVB3 13888 60832 0.36% 0.069% 7 13.195 865 870 875 rBV 7731854 14887663 88.92% 16.951% 8 13.376/ 883 886 893 rVB2 15426 39524 0.24% 0.045% 9 16.548V 1163 1167 1171 rBV 14443 28011 0.17% 0.032% 10 18.343 1319 1326 1331 rBV 7435962 16012475 95.64% 18.231% 11 19.991/ 1467 1472 1481 rVB3 10263 37111 0.22% 0.042% 12 21.334 1585 1591 1595 rBV2 19473 40520 0.24% 0.046% 13 22.283/ 1671 1675 1681 rW2 56233 114077 0.68% 0.130% 14 22.644 1701 1707 1711 rBV2 7143157 16742682 100.00% 19.063% 15 22.768/ 1715 1718 1739 rVB 109344 516072 3.08% 0.588% 16 24.8577 1899 1903 1907 rBV 18013 39500 0.24% 0.045% 17 27.724 2153 2157 2163 rBV 1163143 2132950 12.74% 2.429% 18 30.490 2397 2402 2437 rBV2 5949472 14904128 89.02% 16.969% 19 31.099 2447 2456 2465 rVB6 6809 33561 0.20% 0.038% 20 34.418 2743 2750 2779 rBV 4202592 11849052 70.77% 13.491%

Sum of corrected areas: 87829748

01638.D HP022102.M Mon Feb 25 10:55:49 2002 Page 1

NYC-WTC_000010130

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NYC-WTC_000010130Source: NYC Law Department, mirrored locally

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