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GCMS analysis report for sample AE01509, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01509 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010008–000010026

Folder label: “GCMS X 1/23/02 A 2/21/02

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Scanned page image, NYC-WTC_000010022
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01509 .D Vial: 1 Acq On : 21 Feb 2002 3:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Cyanic acid, ethyl ester $$... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 19.98 0.04 ug/L 30256 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyanic acid, ethyl ester $$ Ethy... 71 C3H5NO 000627-48-5 4 2 Cyanic acid, ethyl ester (CAS) $... 71 C3H5NO 000627-48-5 4 3 Imidazole-2,4,5-d3 $$ IH-Imidazo... 71 C3HD3N2 006745-43-3 4 4 2-Propenamide (CAS) $$ Acrylamid... 71 C3H5NO 000079-06-1 3 Abundance Scan 1471 (19.980 min): 01509.D (-) m/z 71.00 100.00% 71

5000 43 186

19.60 19.80 20.00 20.20 20.40 0-+-1-***1****1***4 1’* . 1 I 1,I I 84 I I I I I | > > I 1 | ! | | ■ I I I I ! | | | ! I | | ! H | 1 ■ ! | | 1 l1 -rp-f m/z 43.10 45.86% niz-> 10 20 30 40 50 60 70 80 90 100110120 130140150 160170 180190 Abundance #1435: Cyanic acid, ethyl ester $$ Ethyl cyanate 29

56 5000 71 19.60 19.80 20.00 20.20 20.40 m/z 186.00 40.20% 0 — . | .... |'l . . | .... | .... ( .... | > l . . | .... | .... | I ... | . ntz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #1436: Cyanic acid, ethyl ester (CAS) $$ Ethyl cyanate 29 1 1 1 ' 1 ' i ■ ‘1**‘I* 56 19.60 19.80 20.00 20.20 20.40 5000 71 rn/z 185.00 32.36%

0- mhmpmmppmmptp iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #1085: Imidazole-2,4,5-d3 $$ 1 H-lmidazole-2,4,5-d3 (CAS) ' i ■ • ■ ■ i ■ ■ ' i 1 ■ 1 1 i 1 71 19.60 19.80 20.00 20.20 20.40 m/z41.10 12.91% 5000 43

0V1,.+agm 1 as 30 ■ i ' ■ ‘ ' i ■ ■ i ■ ■ ■ ■ i ■ ■ ‘ ■ i ■ iz—> 10 2030405060 70 8090 100110120130 140150160170 180190 19.60 19.80 20.00 20.20 20.40

01509.D HP022102.M Mon Feb 25 10:55:04 2002 Page 11

NYC-WTC_000010022

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NYC-WTC_000010022Source: NYC Law Department, mirrored locally

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