GCMS analysis report for sample AE01509, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\1\5973N\02FEB21\01509.D Vial: 1 Acq On : 21 Feb 2002 3:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Flamenol $$ 5-Methoxyresorc... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

13.39 0.07 ug/L 49907 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Flamenol $$ 5-Methoxyresorcinol ... 140 C7H803 002174-64-3 64 2 2,5-Cyclohexadiene- 1,4-dione, 2,... 140 C6H404 000615-94-1 42 3 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 42 4 2-Fluoronicotinamide 140 C6H5FN20 000364-22-7 38 Abundance Scan 887 (13.387 min): 01509.D (-) m/z 140.00 100.00% 1-0 A 5000

43 59 70 TII T TTI

miz-> 0 30 40 50 60 70 I 80 90 100 110 120 130 140 71I 13.00 13.20 13.40 13.60 13.80 m/z 94.00 18.60% Abundance #35376: Flamenol $$ 5-Methoxyresorcinol $$ 3,5-Dihydroxyan... 1-0 111

69 ----- 5000 82 13.00 13.20 13.40 13.60 13.80 97 m/z 70.00 17.38% -.. — miz-> 01 f.T :30 40 50 60 70 80 90 PTI — 100 110 120 130 I........ i.. 140 Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 1-0 TIIt A ‘ ' I ' ‘ ■ I ‘ 13.00 13.20 13.40 13.60 13.80 5000 m/z 43.10 13.06% 42 71 53 84 94 112 .. 1], L +— miz-> O 1 • * 1 * 1

Abundance 30 40 50 60 70 80 90 i ‘ 1 ' ' i 100 110 120 130 #35123:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- ■ ■ I > ‘ I ‘ ‘ - I1' ' " I 140 1-0 TI

m/z r ■ ' ‘ ‘ I 1 1 ' 'I ' ‘ 1 1 1 1 ‘ 13.00 13.20 13.40 13.60 13.80 59.00 MA. 11.57% 42 ft 5000 69

53 84

m/z-> 01 i • ■ ■ 1 i 30 40 . . I.| 50 60 70 1 ■ ।' 80 94 M I 112 90 100 110 120 130 140 2I.I 13.00 13.20 13.40 .13.60 13.80

01509.D HP022102.M Mon Feb 25 10:55:03 2002 Page 9

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